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  A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell

Husband, R. J., Strohm, C., Appel, K., Ball, O. B., Briggs, R., Buchen, J., Cerantola, V., Chariton, S., Coleman, A. L., Cynn, H., Dattelbaum, D., Dwivedi, A., Eggert, J. H., Ehm, L., Evans, W. J., Glazyrin, K., Goncharov, A. F., Graafsma, H., Howard, A., Huston, L., Hutchinson, T. M., Hwang, H., Jacob, S., Kaa, J., Kim, J., Kim, M., Koemets, E., Konôpková, Z., Langenhorst, F., Laurus, T., Li, X., Mainberger, J., Marquardt, H., McBride, E. E., McGuire, C., McHardy, J. D., McMahon, M. I., McWilliams, R. S., Méndez, A. S. J., Mondal, A., Morard, G., O'Bannon, E. F., Otzen, C., Pépin, C. M., Prakapenka, V. B., Prescher, C., Preston, T. R., Redmer, R., Roeper, M., Sanchez-Valle, C., Smith, D., Smith, R. F., Sneed, D., Speziale, S., Spitzbart, T., Stern, S., Sturtevant, B. T., Sztuk-Dambietz, J., Talkovski, P., Velisavljevic, N., Vennari, C., Wu, Z., Yoo, C.-S., Zastrau, U., Jenei, Z., Liermann, H.-P. (2023): A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell. - Journal of Synchrotron Radiation, 30, 4, 671-685.
https://doi.org/10.1107/S1600577523003910

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Husband, Rachel J.1, Author
Strohm, Cornelius1, Author
Appel, Karen1, Author
Ball, Orianna B.1, Author
Briggs, Richard1, Author
Buchen, Johannes1, Author
Cerantola, Valerio1, Author
Chariton, Stella1, Author
Coleman, Amy L.1, Author
Cynn, Hyunchae1, Author
Dattelbaum, Dana1, Author
Dwivedi, Anand1, Author
Eggert, Jon H.1, Author
Ehm, Lars1, Author
Evans, William J.1, Author
Glazyrin, Konstantin1, Author
Goncharov, Alexander F.1, Author
Graafsma, Heinz1, Author
Howard, Alex1, Author
Huston, Larissa1, Author
Hutchinson, Trevor M.1, AuthorHwang, Huijeong1, AuthorJacob, Sony1, AuthorKaa, Johannes1, AuthorKim, Jaeyong1, AuthorKim, Minseob1, AuthorKoemets, Egor1, AuthorKonôpková, Zuzana1, AuthorLangenhorst, Falko1, AuthorLaurus, Torsten1, AuthorLi, Xinyang1, AuthorMainberger, Jona1, AuthorMarquardt, Hauke1, AuthorMcBride, Emma E.1, AuthorMcGuire, Christopher1, AuthorMcHardy, James D.1, AuthorMcMahon, Malcolm I.1, AuthorMcWilliams, R. Stewart1, AuthorMéndez, Alba S. J.1, AuthorMondal, Anshuman1, AuthorMorard, Guillaume1, AuthorO'Bannon, Earl F.1, AuthorOtzen, Christoph1, AuthorPépin, Charles M.1, AuthorPrakapenka, Vitali B.1, AuthorPrescher, Clemens1, AuthorPreston, Thomas R.1, AuthorRedmer, Ronald1, AuthorRoeper, Michael1, AuthorSanchez-Valle, Carmen1, AuthorSmith, Dean1, AuthorSmith, Raymond F.1, AuthorSneed, Daniel1, AuthorSpeziale, S.2, Author              Spitzbart, Tobias1, AuthorStern, Stephan1, AuthorSturtevant, Blake T.1, AuthorSztuk-Dambietz, Jolanta1, AuthorTalkovski, Peter1, AuthorVelisavljevic, Nenad1, AuthorVennari, Cara1, AuthorWu, Zhongyan1, AuthorYoo, Choong-Shik1, AuthorZastrau, Ulf1, AuthorJenei, Zsolt1, AuthorLiermann, Hanns-Peter1, Author more..
Affiliations:
1External Organizations, ou_persistent22              
23.6 Chemistry and Physics of Earth Materials, 3.0 Geochemistry, Departments, GFZ Publication Database, Deutsches GeoForschungsZentrum, ou_146036              

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Free keywords: extreme conditions science, X-ray free-electron lasers, diamond anvil cells, dynamic compression.
 Abstract: An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1.

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Language(s): eng - English
 Dates: 2023-06-152023
 Publication Status: Finally published
 Pages: -
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 Table of Contents: -
 Rev. Type: -
 Identifiers: DOI: 10.1107/S1600577523003910
GFZPOF: keine POF-Zuordnung
OATYPE: Gold Open Access
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Title: Journal of Synchrotron Radiation
Source Genre: Journal, SCI, Scopus, oa , OA ab 2022
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Pages: - Volume / Issue: 30 (4) Sequence Number: - Start / End Page: 671 - 685 Identifier: CoNE: https://gfzpublic.gfz-potsdam.de/cone/journals/resource/journals312
Publisher: Wiley