Novel experimental setup for megahertz X-ray diffraction in a diamond anvil 
cell at the High Energy Density (HED) instrument of the European X-ray 
Free-Electron Laser (EuXFEL)

Liermann, H. P.; Konôpková, Z.; Appel, K.; Prescher, C.; Schropp, A.; Cerantola, V.; Husband, R. J.; McHardy, J. D.; McMahon, M. I.; McWilliams, R. S.; Pépin, C. M.; Mainberger, J.; Roeper, M.; Berghäuser, A.; Damker, H.; Talkovski, P.; Foese, M.; Kujala, N.; Ball, O. B.; Baron, M. A.; Briggs, R.; Bykov, M.; Bykova, E.; Chantel, J.; Coleman, A. L.; Cynn, H.; Dattelbaum, D.; Dresselhaus-Marais, L. E.; Eggert, J. H.; Ehm, L.; Evans, W. J.; Fiquet, G.; Frost, M.; Glazyrin, K.; Goncharov, A. F.; Hwang, H.; Jenei, Zs.; Kim, J.-Y.; Langenhorst, F.; Lee, Y.; Makita, M.; Marquardt, H.; McBride, E. E.; Merkel, S.; Morard, G.; O'Bannon, E. F.; Otzen, C.; Pace, E. J.; Pelka, A.; Pigott, J. S.; Prakapenka, V. B.; Redmer, R.; Sanchez-Valle, C.; Schoelmerich, M.; Speziale, S.; Spiekermann, G.; Sturtevant, B. T.; Toleikis, S.; Velisavljevic, N.; Wilke, M.; Yoo, C.-S.; Baehtz, C.; Zastrau, U.; Strohm, C.

doi:10.1107/S1600577521002551

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Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL)

Authors

Liermann, H. P.
External Organizations;

Konôpková, Z.
External Organizations;

Appel, K.
External Organizations;

Prescher, C.
External Organizations;

Schropp, A.
External Organizations;

Cerantola, V.
External Organizations;

Husband, R. J.
External Organizations;

McHardy, J. D.
External Organizations;

McMahon, M. I.
External Organizations;

McWilliams, R. S.
External Organizations;

Pépin, C. M.
External Organizations;

Mainberger, J.
External Organizations;

Roeper, M.
External Organizations;

Berghäuser, A.
External Organizations;

Damker, H.
External Organizations;

Talkovski, P.
External Organizations;

Foese, M.
External Organizations;

Kujala, N.
External Organizations;

Ball, O. B.
External Organizations;

Baron, M. A.
External Organizations;

Briggs, R.
External Organizations;

Bykov, M.
External Organizations;

Bykova, E.
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Chantel, J.
External Organizations;

Coleman, A. L.
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Cynn, H.
External Organizations;

Dattelbaum, D.
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Dresselhaus-Marais, L. E.
External Organizations;

Eggert, J. H.
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Ehm, L.
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Evans, W. J.
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Fiquet, G.
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Frost, M.
External Organizations;

Glazyrin, K.
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Goncharov, A. F.
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Hwang, H.
External Organizations;

Jenei, Zs.
External Organizations;

Kim, J.-Y.
External Organizations;

Langenhorst, F.
External Organizations;

Lee, Y.
External Organizations;

Makita, M.
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Marquardt, H.
External Organizations;

McBride, E. E.
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Merkel, S.
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Morard, G.
External Organizations;

O'Bannon, E. F.
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Otzen, C.
External Organizations;

Pace, E. J.
External Organizations;

Pelka, A.
External Organizations;

Pigott, J. S.
External Organizations;

Prakapenka, V. B.
External Organizations;

Redmer, R.
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Sanchez-Valle, C.
External Organizations;

Schoelmerich, M.
External Organizations;

/persons/resource/speziale

Speziale, S.
3.6 Chemistry and Physics of Earth Materials, 3.0 Geochemistry, Departments, GFZ Publication Database, Deutsches GeoForschungsZentrum;

Spiekermann, G.
External Organizations;

Sturtevant, B. T.
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Toleikis, S.
External Organizations;

Velisavljevic, N.
External Organizations;

Wilke, M.
External Organizations;

Yoo, C.-S.
External Organizations;

Baehtz, C.
External Organizations;

Zastrau, U.
External Organizations;

Strohm, C.
External Organizations;

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5006926.pdf
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Citation

Liermann, H. P., Konôpková, Z., Appel, K., Prescher, C., Schropp, A., Cerantola, V., Husband, R. J., McHardy, J. D., McMahon, M. I., McWilliams, R. S., Pépin, C. M., Mainberger, J., Roeper, M., Berghäuser, A., Damker, H., Talkovski, P., Foese, M., Kujala, N., Ball, O. B., Baron, M. A., Briggs, R., Bykov, M., Bykova, E., Chantel, J., Coleman, A. L., Cynn, H., Dattelbaum, D., Dresselhaus-Marais, L. E., Eggert, J. H., Ehm, L., Evans, W. J., Fiquet, G., Frost, M., Glazyrin, K., Goncharov, A. F., Hwang, H., Jenei, Z., Kim, J.-Y., Langenhorst, F., Lee, Y., Makita, M., Marquardt, H., McBride, E. E., Merkel, S., Morard, G., O'Bannon, E. F., Otzen, C., Pace, E. J., Pelka, A., Pigott, J. S., Prakapenka, V. B., Redmer, R., Sanchez-Valle, C., Schoelmerich, M., Speziale, S., Spiekermann, G., Sturtevant, B. T., Toleikis, S., Velisavljevic, N., Wilke, M., Yoo, C.-S., Baehtz, C., Zastrau, U., Strohm, C. (2021): Novel experimental setup for megahertz X-ray diffraction in a diamond anvil cell at the High Energy Density (HED) instrument of the European X-ray Free-Electron Laser (EuXFEL). - Journal of Synchrotron Radiation, 28, 688-706.
https://doi.org/10.1107/S1600577521002551

Cite as: https://gfzpublic.gfz-potsdam.de/pubman/item/item_5006926

Abstract

The high-precision X-ray diffraction setup for work with diamond anvil cells (DACs) in interaction chamber 2 (IC2) of the High Energy Density instrument of the European X-ray Free-Electron Laser is described. This includes beamline optics, sample positioning and detector systems located in the multipurpose vacuum chamber. Concepts for pump-probe X-ray diffraction experiments in the DAC are described and their implementation demonstrated during the First User Community Assisted Commissioning experiment. X-ray heating and diffraction of Bi under pressure, obtained using 20 fs X-ray pulses at 17.8 keV and 2.2 MHz repetition, is illustrated through splitting of diffraction peaks, and interpreted employing finite element modeling of the sample chamber in the DAC.