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Journal Article

A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell

Authors

Husband,  Rachel J.
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Strohm,  Cornelius
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Appel,  Karen
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Ball,  Orianna B.
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Briggs,  Richard
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Buchen,  Johannes
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Cerantola,  Valerio
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Chariton,  Stella
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Coleman,  Amy L.
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Cynn,  Hyunchae
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Dattelbaum,  Dana
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Dwivedi,  Anand
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Eggert,  Jon H.
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Ehm,  Lars
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Evans,  William J.
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Glazyrin,  Konstantin
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Goncharov,  Alexander F.
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Graafsma,  Heinz
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Howard,  Alex
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Huston,  Larissa
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Hutchinson,  Trevor M.
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Hwang,  Huijeong
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Jacob,  Sony
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Kaa,  Johannes
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Kim,  Jaeyong
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Kim,  Minseob
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Koemets,  Egor
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Konôpková,  Zuzana
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Langenhorst,  Falko
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Laurus,  Torsten
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Li,  Xinyang
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Mainberger,  Jona
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Marquardt,  Hauke
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McBride,  Emma E.
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McGuire,  Christopher
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McHardy,  James D.
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McMahon,  Malcolm I.
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McWilliams,  R. Stewart
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Méndez,  Alba S. J.
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Mondal,  Anshuman
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Morard,  Guillaume
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O'Bannon,  Earl F.
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Otzen,  Christoph
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Pépin,  Charles M.
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Prakapenka,  Vitali B.
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Prescher,  Clemens
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Preston,  Thomas R.
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Redmer,  Ronald
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Roeper,  Michael
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Sanchez-Valle,  Carmen
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Smith,  Dean
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Smith,  Raymond F.
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Sneed,  Daniel
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/persons/resource/speziale

Speziale,  S.
3.6 Chemistry and Physics of Earth Materials, 3.0 Geochemistry, Departments, GFZ Publication Database, Deutsches GeoForschungsZentrum;

Spitzbart,  Tobias
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Stern,  Stephan
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Sturtevant,  Blake T.
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Sztuk-Dambietz,  Jolanta
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Talkovski,  Peter
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Velisavljevic,  Nenad
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Vennari,  Cara
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Wu,  Zhongyan
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Yoo,  Choong-Shik
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Zastrau,  Ulf
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Jenei,  Zsolt
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Liermann,  Hanns-Peter
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External Ressource
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Fulltext (public)

5022834.pdf
(Publisher version), 2MB

Supplementary Material (public)
There is no public supplementary material available
Citation

Husband, R. J., Strohm, C., Appel, K., Ball, O. B., Briggs, R., Buchen, J., Cerantola, V., Chariton, S., Coleman, A. L., Cynn, H., Dattelbaum, D., Dwivedi, A., Eggert, J. H., Ehm, L., Evans, W. J., Glazyrin, K., Goncharov, A. F., Graafsma, H., Howard, A., Huston, L., Hutchinson, T. M., Hwang, H., Jacob, S., Kaa, J., Kim, J., Kim, M., Koemets, E., Konôpková, Z., Langenhorst, F., Laurus, T., Li, X., Mainberger, J., Marquardt, H., McBride, E. E., McGuire, C., McHardy, J. D., McMahon, M. I., McWilliams, R. S., Méndez, A. S. J., Mondal, A., Morard, G., O'Bannon, E. F., Otzen, C., Pépin, C. M., Prakapenka, V. B., Prescher, C., Preston, T. R., Redmer, R., Roeper, M., Sanchez-Valle, C., Smith, D., Smith, R. F., Sneed, D., Speziale, S., Spitzbart, T., Stern, S., Sturtevant, B. T., Sztuk-Dambietz, J., Talkovski, P., Velisavljevic, N., Vennari, C., Wu, Z., Yoo, C.-S., Zastrau, U., Jenei, Z., Liermann, H.-P. (2023): A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell. - Journal of Synchrotron Radiation, 30, 4, 671-685.
https://doi.org/10.1107/S1600577523003910


Cite as: https://gfzpublic.gfz-potsdam.de/pubman/item/item_5022834
Abstract
An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1.